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Extracting salvinorin a from sage of the diviners

chemistrydude

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Salvinarin A structure scheme

For extraction you need flask, and extractor.
Putting into flask 450ml of ethyl alcohol, and installing the exctractor on the flask, you need to put into extractor the sage of diviners and 155ml of ethyl alcohol again, and start the extraction.
When all was extracted you get oil, time for make mixture.
Putting the 55 grams of NaOH(sodium hydroxide), and adding 255ml of water, now mix it, and put NaOH into oil it will start crystalyizing, after that proccess about 6 hours you need put into crystalized oil the amyl bromid about 57ml, mix it, and put on plate the temerature 85*C, about 25 minutes and done, filtrate you're product, now wash it in isopropyl alcohol, and put in bowl to dry you're product.
Done hope it helped you!
 
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