BK-MDMA SYNTHESIS EASY AND FAST METHOD.

[Acidosis]

The free base in into the cube brown-yellow

 

[hider8028]

The free base in into the cube brown-yellow

AcidosisCan you provide me with suppliers who sell methylamine 40% and 36% HCL?

 

[Precursor-supplier]

Can you provide me with suppliers who sell methylamine 40% and 36% HCL?

hider8028methylamine 40% Contact me

 

[Acidosis]

Final process from 500g of 2b3'4mp 390g pure Brown cola crystals of BK-MDMA.

 

[hider8028]

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[alquimista00]

Final process from 500g of 2b3'4mp 390g pure Brown cola crystals of BK-MDMA.

Acidosishow can i make coca cola from mdma base??
and i would like to know what is the difference bk-mdma and normal mdma??

 

[hider8028]

boss i need help make bk-mdma
Are you willing to provide a detailed raw material list and make a production video? I am willing to pay for it! I hope to get your help

 

[antrax]

boss i need help make bk-mdma
Are you willing to provide a detailed raw material list and make a production video? I am willing to pay for it! I hope to get your help

hider8028It is a simple and fast synthesis route.
The chemicals you need are the following: the chemical precursor (CAS:52190-28-0),DCM, Methylamine 40% aqueous solution, Ethyl acetate, Distilled water, HCl 35-38%, Pure acetone, Deionized water.

 

[41Dxflatline]

Just gonna leave this here: https://en.wikipedia.org/wiki/Wolff–Kishner_reduction

 

[hider8028]

Hello, here I attach a simple and simple synthesis of bkmdma with photos of the process and the finished product.
1-To begin with, two plastic drums of approximately 25 liters were brought and inside a drum, an exact 500g of C.A.S: 52190-28-0 of excellent quality was dissolved in 2.5 liters of DCM (dichloromethane) and with an electric drill with a bit mixing concrete was stirred until the complete dissolution of the precursor, this did not take more than a few minutes.

2- now added 1litre of methylamine in in different portions at the rate of 250ml every 10 minutes approximately. At no time was the temperature increase noted since all the reagents were cold before starting, at no time was heat used for this reaction. once all the methylamine was added it was allowed to stir for 40 minutes until no more methylamine gas fumes were observed.

3- 50 minutes after the beginning of the reaction, the agitation was stopped and we waited a few minutes until the 2 layers were separated: the base and and the aqueous layer formed from methylamine and still traces of product, for this another plastic drum was used and the layer The aqueous layer was separated to the new drum for its subsequent extractions of some of the product that remained in the aqueous layer. For this, ethyl acetate was used. 100 milliliters of ethyl acetate were added three times each time to the aqueous layer and it was collected to add it. to the other tambo where the base was reserved.

4- Once the 3 extractions were united with the base in the same drum, the base was cleaned, for this abundant water was added and stirred together with the base and once the water was separated, all the water was emptied from the other drum thus leaving the clean methylone base in the first tube. This cleaning process was repeated at least 3 times until the base did not give off any smell of methylamine. Now a good handful of magnesium sulfate was added to the drum that contained the base and it was left to dry for 20 minutes, during which time it was used to get rid of the cleaning of water deposited in the other bucket. As can be seen, the entire synthesis is being carried out only with the help of 2 plastic buckets and a normal masonry drill with a bit to mix the mortar and cement and with a good source of water near the production area.


5- formation of methylone hydrochloride, for this, sufficient 36% HCL was prepared in a beaker with a little cold acetone, once again the electric drill was turned on and the base was constantly stirred and the hcl was added in small portions and measure the ph until reaching ph 5, at that moment they stopped adding more HCL but the base was kept stirring for a little longer, when we stopped the drill we observed a lot of hydrochloride both floating and on the walls, the bottom of the cube and attached to the drill .


6- filtration process. For this, the other cube was taken again and a filter was placed on top of it, firmly attached with tweezers and all the solution was filtered, leaving the methylone trapped in the filter. The cube and the hole that contained methylone were scraped and drained well. it was ignited and air dried to yield 90% dry of the actual weight of precursor.


7- recristalization . 490g of Methylone HCL were put to recrystallization with water and acetone in the proportion of: for each gram of HCL 1.5ml of distilled water and 1ml of acetone which formed some beautiful crystals and at the same time purified its purity to reach a good percentage of pure bkmdma crystal.

AcidosisBoss, since I am a novice, I want to know clearly the amount of acetone and36% HCL, and the amount of magnesium sulfate
thank you very much boss

 

[hider8028]

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[antrax]

Boss, since I am a novice, I want to know clearly the amount of acetone and36% HCL, and the amount of magnesium sulfate
thank you very much boss

hider8028There is no exact amount of HCl & pure acetone solution that you should add to the organic base, you must add the solution little by little to the organic base with the help of a pipette until the pH reaches 5 and you will see that it begins to come out Methylone HCl.
magnesium sulfate is not mandatory (optional only).

 

[hider8028]

There is no exact amount of HCl & pure acetone solution that you should add to the organic base, you must add the solution little by little to the organic base with the help of a pipette until the pH reaches 5 and you will see that it begins to come out Methylone HCl.
magnesium sulfate is not mandatory (optional only).

antraxThank you very much boss

 

[/\/\1]

@Acidosis
will 33% HCL solution work too? or do i need to make it stronger by evaporation or something?

edit: also in the beautiful pictures you show your fingers and fingerprints be careful my friend!

 

[antrax]

@Acidosis
will 33% HCL solution work too? or do i need to make it stronger by evaporation or something?

edit: also in the beautiful pictures you show your fingers and fingerprints be careful my friend!

/\/\1A lower concentration of HCl also works, but you must add more solution than a higher concentration.
since HCI 33% does not have the same acidity as, for example, HCI 38%

 

[craris100]

Hi, you are using 40% Methylamine in water or in Methanol?. Thank you.

 

[antrax]

Hi, you are using 40% Methylamine in water or in Methanol?. Thank you.

craris100in water,in methanol for MDMA