BK-MDMA SYNTHESIS EASY AND FAST METHOD.

[Acidosis]

Final process from 500g of 2b3'4mp 390g pure Brown cola crystals of BK-MDMA.

 

[lalosalamanca84]

Final process from 500g of 2b3'4mp 390g pure Brown cola crystals of BK-MDMA.

Acidosissomebody try make extasy pills from bk-mdma? what dosage is enought to put in 1 pill...?

 

[cartelloszetas]

Feebasse i have on top

 

[wavyUK]

Feebasse i have on top

cartelloszetasPls can you pm me

 

[antrax]

 

[PolandoEmingarnte]

View attachment 18676

antraxhow much gram crystal no powder u get form 100g 2b34m ?

 

[antrax]

how much gram crystal no powder u get form 100g 2b34m ?

PolandoEmingarntei don´t know, i got 8,5 grams powder from 10 grams of precursor.

 

[antrax]

View attachment 18676

antraxi started with 10 grams of precursor (CAS 52190-28-0) which I dissolved with 50ml DCM, then mixed well by hand with a spoon until precursor was properly dissolved, then added 20ml methylamine 40% aqueous solution to the dissolved precursor and in a very short period after mixing with the spoon by hand 2 layers were formed, I separated the aqueous layer from the base with the help of a pipette and added 6ml of ethyl acetate to the aqueous layer after mixing for a short period of time I added again the aqueous layer that I mixed with ethyl acetate to the base, then I added 10ml of water to the base to wash it and I stirred it until 2 layers were formed, but before adding the water the 2 layers were also formed, after removing the aqueous layer of the base i added 2 grams of magnesium sulphate and let it dry for a while, then i checked the pH and it was 7, then i made a 9ml solution of 35-38% lab grade hydrochloric acid with 1ml of acetone and mixed it well, then I added the solution drop by drop to the base and checked the pH each time, and it was still at 7 and then I added a little more solution and the pH was less than 1, instead it should be 5 ,5. In total I added about 5ml of the solution, and I exceeded the quantity, then I took filter paper, filtered it and supposedly left the methylone hydrochloride dry, then I took a methylone anti-drug test and I think it was not positive, no idea.

 

[blosuetoday]

but you can appreciate the color of the drug test, it doesn't seem to be red as indicated for methylone positive, rather brown.

antraxRed? I only see that you need brown color and you got it.

 

[antrax]

now I will have to wait several days until crystals form.

 

[Heineken]

now I will have to wait several days until crystals form.

antraxnormal is 1 day to made crystal

 

[antrax]

normal is 1 day to made crystal

HeinekenI also believe too that my chemical precursor (CAS: 52190-28-0) is impure and dirty.
According to the Chinese supplier, it has a purity of 99%, but I think he deceived me, how can I know, that is, to ask him for some laboratory document, in which he reports that said chemical precursor has that percentage of purity.

 

[lalosalamanca84]

Pozdrav, ovdje prilažem jednostavnu i jednostavnu sintezu bkmdma sa fotografijama procesa i gotovog proizvoda.
1-Za početak su dovedene dvije plastične bačve od cca 25 litara i unutar bubnja je u 2,5 litara DCM (dihlorometana) i električnom bušilicom rastvoreno tačno 500 g CAS: 52190-28-0 odličnog kvaliteta. malo se miješajući beton miješa do potpunog rastvaranja prethodnika, za to nije trebalo više od nekoliko minuta.

2- sada dodaje 1 litar metilamina u različitim porcijama brzinom od 250 ml svakih 10 minuta otprilike. Ni u jednom trenutku nije zabilježeno povećanje temperature jer su svi reagensi bili hladni prije pokretanja, niti u jednom trenutku nije korištena toplina za ovu reakciju. nakon što je dodat sav metilamin, ostavljeno je da se miješa 40 minuta dok se više ne primjećuju isparenja plina metilamina.

3-50 minuta nakon početka reakcije, miješanje je zaustavljeno i čekali smo nekoliko minuta dok se ne razdvoje 2 sloja: baza i vodeni sloj formiran od metilamina i još tragova proizvoda, za ovaj drugi plastični bubanj Korišteni i sloj Vodeni sloj je odvojen u novi bubanj za njegovu naknadnu ekstrakciju dijela proizvoda koji je ostao u vodenom sloju. Za to je korišten etil acetat. 100 mililitara etil acetata je svaki put dodano tri puta u vodeni sloj i on je sakupljen za dodavanje. na drugi tambo gdje je baza bila rezervisana.

4- Nakon što su 3 ekstrakcije sjedinjene sa bazom u istom bubnju, baza je očišćena, jer je ova voda u izobilju dodana i promešana zajedno sa bazom i kada je voda odvojena, sva voda je ispražnjena iz drugog bubnja. ostavljajući čistu metilonsku bazu u prvoj epruveti. Ovaj proces čišćenja je ponovljen najmanje 3 puta dok baza nije ispuštala nikakav miris metilamina. Sada je dobra šaka magnezijum sulfata dodana u bubanj u kojem je bila baza i ostavljena da se suši 20 minuta, a za to vrijeme je korištena da se riješi čišćenje vode koja se taložila u drugoj kanti. Kao što se može vidjeti, cjelokupna sinteza se izvodi samo uz pomoć 2 plastične kante i normalne bušilice za zidanje sa malom za miješanje maltera i cementa i uz dobar izvor vode u blizini proizvodnog prostora.


5- formiranje metilon hidrohlorida, za to je pripremljeno dovoljno 36% HCL u čaši sa malo hladnog acetona, još jednom je uključena električna bušilica i baza je stalno mešana i dodavan hcl u malim porcijama i merenje ph do ph 5, u tom trenutku su prestali dodavati još HCL ali se baza još malo miješala, kada smo zaustavili bušilicu primijetili smo dosta hidroklorida kako pluta i na zidovima, dnu kocke i pričvršćenim na bušilicu.


6- proces filtracije. Za to je ponovo uzeta druga kocka i na nju je postavljen filter, čvrsto pričvršćen pincetom i sav rastvor je filtriran, ostavljajući metilon zarobljen u filteru. Kocka i rupa koja je sadržavala metilon su ostrugana i dobro ocijeđena. zapaljen je i osušen na vazduhu da bi se dobilo 90% suvog od stvarne težine prekursora.


7- rekristalizacija . 490g metilona HCL stavljeno je na rekristalizaciju sa vodom i acetonom u omjeru: za svaki gram HCL 1,5ml destilovane vode i 1ml acetona koji je formirao prelijepe kristale i istovremeno pročišćavao svoju čistoću da bi dostigao dobar postotak čisti bkmdma kristal.

Acidosisdo you can please put all reagens calculation exactly?

 

[Goku]

do you can please put all reagens calculation exactly?

lalosalamanca84u have look good

 

[antrax]

i started with 100 grams of precursor (CAS: 52190-28-0) 500ml of DCM, 200ml of methylamine 40% aqueous solution, 60ml of ethyl acetate, 300ml of distilled water in total for (wash the base 3 times) a solution of HCI 35-38% lab grade & pure acetone (didn't add too much solution) (pH wasn't 5 it was 6-7-8) then I got about 51 grams of methylone hydrochloride, then I got about 60ml of acetone and about 80ml of distilled water and I added it to the beaker along with the 51 grams of methylone hydrochloride and recrystallized them, for about 10 hours, it may not have done the crystallization process well either, but I can see that the powder has a lot of Micro crystals that shine when you shine a flashlight on them.

 

[PolandoEmingarnte]

i started with 100 grams of precursor (CAS: 52190-28-0) 500ml of DCM, 200ml of methylamine 40% aqueous solution, 60ml of ethyl acetate, 300ml of distilled water in total for (wash the base 3 times) a solution of HCI 35-38% lab grade & pure acetone (didn't add too much solution) (pH wasn't 5 it was 6-7-8) then I got about 51 grams of methylone hydrochloride, then I got about 60ml of acetone and about 80ml of distilled water and I added it to the beaker along with the 51 grams of methylone hydrochloride and recrystallized them, for about 10 hours, it may not have done the crystallization process well either, but I can see that the powder has a lot of Micro crystals that shine when you shine a flashlight on them.
View attachment 19897

antraxif u made crystal like ice u can lost 20% or more then will be pure.
This what u get it still powder

 

[antrax]

if u made crystal like ice u can lost 20% or more then will be pure.
This what u get it still powder

PolandoEmingarnteheineken u again? u change account every time

 

[PolandoEmingarnte]

i started with 100 grams of precursor (CAS: 52190-28-0) 500ml of DCM, 200ml of methylamine 40% aqueous solution, 60ml of ethyl acetate, 300ml of distilled water in total for (wash the base 3 times) a solution of HCI 35-38% lab grade & pure acetone (didn't add too much solution) (pH wasn't 5 it was 6-7-8) then I got about 51 grams of methylone hydrochloride, then I got about 60ml of acetone and about 80ml of distilled water and I added it to the beaker along with the 51 grams of methylone hydrochloride and recrystallized them, for about 10 hours, it may not have done the crystallization process well either, but I can see that the powder has a lot of Micro crystals that shine when you shine a flashlight on them.
View attachment 19897

antrax51% powder is no too much very good chemist get 95% powder
like say hang schneider

 

[PolandoEmingarnte]

synthesize 2b34m yourself, your costs for the precursor will be less and you will have a lot of cleaners. Thus, the efficiency after 2 dcm does not mix and heats for 2 hours at 40 °. same toluene in 2h at 60° after 3 you can see by the color of the powder that it still contains a lot of impurities. after 4 the crystallization of the ice crystal takes up to 2 weeks and then it is a real glass non-crystalline powder

 

[PolandoEmingarnte]

 

[antrax]

I have obtained 7.25 grams of methylone HCI starting with 10 grams of precursor CAS 52190-28-0, the pH was 5, after adding the HCI & acetone solution to the organic base, the yield is (72.5%) very low, since the user @Acidosis who shared said bk-MDMA chemical synthesis route says that 90% yield is obtained from the precursor CAS 52190-28-0.

 

[wavyUK]

I have obtained 7.25 grams of methylone HCI starting with 10 grams of precursor CAS 52190-28-0, the pH was 5, after adding the HCI & acetone solution to the organic base, the yield is (72.5%) very low, since the user @Acidosis who shared said bk-MDMA chemical synthesis route says that 90% yield is obtained from the precursor CAS 52190-28-0.

antraxHas it been recrystallized ?

 

[antrax]

Has it been recrystallized ?

wavyUKnah bruh, that's just the methylone HCI (powder) if I recrystallize it the yield will be even lower.

 

[wavyUK]

nah bruh, that's just the methylone HCI (powder) if I recrystallize it the yield will be even lower.

antraxIs it usable in its current state

 

[antrax]

Is it usable in its current state

wavyUKOf course it can be consumed, but it has or may have impurities and by recrystallizing it we would eliminate these impurities so that the final product would be purer and would have more effect.

 

[wavyUK]

Of course it can be consumed, but it has or may have impurities and by recrystallizing it we would eliminate these impurities so that the final product would be purer and would have more effect.

antraxDid ur precursor look same as acidosis or was it that dark brown type do u think this could be the reason for low yield

 

[antrax]

Did ur precursor look same as acidosis or was it that dark brown type do u think this could be the reason for low yield

wavyUKIt´s the same, i already asked him.