Ephedrone synthesis in DCM solvent using Potassium permanganate

[DrugZ]

Methcathinone synthesis by DrugZ
1. Smash pseudoephedrine (for example 360mg) pills into fine powder
2. Take a jar and put 50ml distilled water and 2.5ml acetic acid.
3. Put the pseudoephedrine powder into jar filled with distilled water, put the cap on and shake very well to dissolve pseudoephedrine.
4. Get another jar and 1 coffee filter, filter first jar to second one to get any left undissolved pseudoephedrine.
5. Calculate your kMNO4 to 300-360mg and mix with pseudoedephrine filled jar.
6. The reaction has started and should take 20-30 minutes to reach its final destination.
7. After mentioned time, reaction should have ended and you have to see brown particles by swirling the jar, if there's no brown coffee like particles that means reaction hasn't finished and you need to wait for a bit more. You should see clear water at the top but if you add to much kMNO4 you need to swirl jar and see if there is any brown particles.
8. Add some sodium sulfite (not NaOH, it is strong lye and methcathinone is sensitive to strong lyes, it will destroy your yield)until you reach pH of 8-9, then you should notice clear liquid turn into yellow color and the smell should change).
9. Put the cap on jar and shake very well for 1 minute.
10. Get another coffee filter, jar and filter it out, there should not be any brown particles left only yellow liquid (the methcathinone).
11. Next step is to add 36ml of methylene chloride (DCM) stir or it up and let it settle for bit till it separates into 2 layers (organic - bottom and aqueous one - on top) suck off top layer with turkey baster or whatever comes in your mind to do it well.
12. Exract aqueous phase 3 times more with 9ml DCM and combine all DCM
How to crystallize comment, if I'm somewhere wrong correct me, thanks.

 

[DrugZ]

This method is not finished and I need your help in comments

 

[DrugZ]

Methcathinone synthesis by DrugZ
1. Smash pseudoephedrine (for example 360mg) pills into fine powder
2. Take a jar and put 50ml distilled water and 2.5ml acetic acid.
3. Put the pseudoephedrine powder into jar filled with distilled water, put the cap on and shake very well to dissolve pseudoephedrine.
4. Get another jar and 1 coffee filter, filter first jar to second one to get any left undissolved pseudoephedrine.
5. Calculate your kMNO4 to 300-360mg and mix with pseudoedephrine filled jar.
6. The reaction has started and should take 20-30 minutes to reach its final destination.
7. After mentioned time, reaction should have ended and you have to see brown particles by swirling the jar, if there's no brown coffee like particles that means reaction hasn't finished and you need to wait for a bit more. You should see clear water at the top but if you add to much kMNO4 you need to swirl jar and see if there is any brown particles.
8. Add some sodium sulfite (not NaOH, it is strong lye and methcathinone is sensitive to strong lyes, it will destroy your yield)until you reach pH of 8-9, then you should notice clear liquid turn into yellow color and the smell should change).
9. Put the cap on jar and shake very well for 1 minute.
10. Get another coffee filter, jar and filter it out, there should not be any brown particles left only yellow liquid (the methcathinone).
11. Next step is to add 36ml of methylene chloride (DCM) stir or it up and let it settle for bit till it separates into 2 layers (organic - bottom and aqueous one - on top) suck off top layer with turkey baster or whatever comes in your mind to do it well.
12. Exract aqueous phase 3 times more with 9ml DCM and combine all DCM
How to crystallize comment, if I'm somewhere wrong correct me, thanks.

DrugZSmall Methcathinone part will remain in the lower organic layer, the main part will be in water.
Step 8. pH needs to be lower than 10 but not lower than 8.

Do not try to drink too much you can die and im not responsible for this, try to add one or few drops to tea and see if you can see the difference and it gets you high.

 

[G.Patton]

Hello. As I already told in this topic https://bbgate.com/threads/5-minute-methcathinone-synthesis-from-pseudoephedrine.716 , I think this method isn't work.

 

[DrugZ]

Yes the method you included wont work, you need lye to reach pH 8-10 and DCM (Methylene Chloride). To crystallize it you need to reach pH of 5 with HCL 36-38% then evaporate till its like oily stuff going in and then put it in freezer till you see crystals. Evaporate as much water as you can, like i said till you see color change and it is oily.

 

[strannik]

Methcathinone synthesis by DrugZ
1. Smash pseudoephedrine (for example 360mg) pills into fine powder
2. Take a jar and put 50ml distilled water and 2.5ml acetic acid.
3. Put the pseudoephedrine powder into jar filled with distilled water, put the cap on and shake very well to dissolve pseudoephedrine.
4. Get another jar and 1 coffee filter, filter first jar to second one to get any left undissolved pseudoephedrine.
5. Calculate your kMNO4 to 300-360mg and mix with pseudoedephrine filled jar.
6. The reaction has started and should take 20-30 minutes to reach its final destination.
7. After mentioned time, reaction should have ended and you have to see brown particles by swirling the jar, if there's no brown coffee like particles that means reaction hasn't finished and you need to wait for a bit more. You should see clear water at the top but if you add to much kMNO4 you need to swirl jar and see if there is any brown particles.
8. Add some sodium sulfite (not NaOH, it is strong lye and methcathinone is sensitive to strong lyes, it will destroy your yield)until you reach pH of 8-9, then you should notice clear liquid turn into yellow color and the smell should change).
9. Put the cap on jar and shake very well for 1 minute.
10. Get another coffee filter, jar and filter it out, there should not be any brown particles left only yellow liquid (the methcathinone).
11. Next step is to add 36ml of methylene chloride (DCM) stir or it up and let it settle for bit till it separates into 2 layers (organic - bottom and aqueous one - on top) suck off top layer with turkey baster or whatever comes in your mind to do it well.
12. Exract aqueous phase 3 times more with 9ml DCM and combine all DCM
How to crystallize comment, if I'm somewhere wrong correct me, thanks.

DrugZYou can get manganese encephalopathy. Toxic encephalopathy is the death of brain cells due to exposure to toxic substances. Toxic manganese encephalopathy usually develops after consuming the artisanal drug Ephedron ("Mulka", "Jeff", etc.) containing manganese. Manganese is deposited in certain structures of the brain (subcortical nuclei) and destroys them. Subcortical nuclei are the regulator of muscle tone, postures and movements. The death of subcortical nuclei is accompanied by parkinsonism, in this case – "manganese parkinsonism".