Dear Mr.
Use L tartaric acid to separate the free base according to your method.
I got a chewing gum-like substance while stirring, and once I stopped stirring everything turned into a very hard white solid. A whole piece.
Is this correct?
Use L tartaric acid to separate the free base according to your method.
I got a chewing gum-like substance while stirring, and once I stopped stirring everything turned into a very hard white solid. A whole piece.
Is this correct?
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Dear Mr.
Use L tartaric acid to separate the free base according to your method.
I got a chewing gum-like substance while stirring, and once I stopped stirring everything turned into a very hard white solid. A whole piece.
Is this correct?
↑View previous replies…
qwe111It won't turn liquid the liquid is mixed with the hard solid you must crush it to vacuum filtration and get the liquid.
About freebase yield from p2p is ok if not steam distilled p2p used.
btcboss2022Dear Mr.
I used L tartaric acid to separate the free base. Vacuum gives liquid. Alkaline PH-13. Free base is obtained.
Stir the free base. Join HCI. PH value -2. I wanted to adjust the pH to -3. But the pH suddenly dropped. I'm careful to add very little HCI. The pH value has always been around 7 in the beginning. Then suddenly it drops to -2.
Heat to 130°. Pour into a container with 10 volumes of chilled isopropyl alcohol. A lot of powder immediately appeared in the container. Shouldn't we get crystals?
What did I do wrong?
Sir, please help me.
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- By btcboss2022
sorry sir.
I'm a beginner. I followed your lead on the forum and synthesized.
From 5449~p2p I use the phosphoric acid method you shared. It worked the first time. Got a nice looking orange p2p.
From p2p ~ methamphetamine free base I used the sodium borohydride synthesis method you shared. It failed 2 times before. Later I got a light yellow oil. I don't know if he was methamphetamine freebase.
I followed exactly the method you shared.
Yesterday I used this oil. Follow the L tartaric acid separation you shared.
More than ten hours have passed now. It's very hard. Like ice cream in the freezer. There is no liquid present.
I'm very confused and worried right now.
Will it turn liquid after 24 hours?
About freebase yield from p2p is ok if not steam distilled p2p used.
It won't turn liquid the liquid is mixed with the hard solid you must crush it to vacuum filtration and get the liquid.
About freebase yield from p2p is ok if not steam distilled p2p used.
I used L tartaric acid to separate the free base. Vacuum gives liquid. Alkaline PH-13. Free base is obtained.
Stir the free base. Join HCI. PH value -2. I wanted to adjust the pH to -3. But the pH suddenly dropped. I'm careful to add very little HCI. The pH value has always been around 7 in the beginning. Then suddenly it drops to -2.
Heat to 130°. Pour into a container with 10 volumes of chilled isopropyl alcohol. A lot of powder immediately appeared in the container. Shouldn't we get crystals?
What did I do wrong?
Sir, please help me.